Organic syntheses. V. 56

Автор(ы):Журнал
06.10.2007
Год изд.:1977
Описание: Пятьдесят шестой номер брошюры «Органический синтез» содержит описание следующих соединений: 5-ACETYL-1,2,3,4,5-PENTAMETHYLCYOLOPENTADIENE; ACYLAMIDOALKYL ACETOPHENONES FRОМ SUBSTITUTED PHENETHYLAMINES: 2-(2-ACETAMIDOETHYL)-4,5-DIMETHOXYACETOPHENONE; 3-ALKYLATED AND 3-ACYLATED INDOLES FROM A COMMON PRECURSOR: 3-BENZYLINDOLE AND 3-BENZOYLINDOLE; ortho-ALKYLATION OF ANILINES: ETHYL 4-AMINO-3-METHYLBENZOATE; ALKYLATION OF ISOQUINOLINE via 2-BENZOYL-1,2-DIHYDROISOQUINALDONITRILES: 1-BENZYLISOQUINOLINE; ALLYLIC OXIDATION WITH HYDROGEN PEROXIDE-SELENIUM DIOXIDE: trans-PINOCARVEOL; CARBOXYLATION OF AROMATIC COMPOUNDS: FERBOCENECARBOXYLIC ACID; CHAIN ELONGATION OP ALKENES via gem-DIHALOCYCLOPROPANES: 1,1-DIPHENYL-2-BROMO-3-ACETOXY-1-PROPENE; CONVERSION OF NITRO то CARBONYL BY OZONOLYSIS OF NITRONATES: 2,5-HEPTANEDIONE. А также некоторые другие. Всего рассмотрено 27 соединений.
Оглавление:
Organic syntheses. V. 56 — обложка книги.
5 ACETYL-1,2,3,4,5-PENTAMETHYLCYOLOPENTADIENE [1]
ACYLAMIDOALKYL ACETOPHENONES FRОМ SUBSTITUTED PHENETHYLAMINES: 2-(2-ACETAMIDOETHYL)-4,5-DIMETHOXYACETOPHENONE [3]
3-ALKYLATED AND 3-ACYLATED INDOLES FROM A COMMON PRECURSOR: 3-BENZYLINDOLE AND 3-BENZOYLINDOLE [8]
ortho-ALKYLATION OF ANILINES: ETHYL 4-AMINO-3-METHYLBENZOATE [15]
ALKYLATION OF ISOQUINOLINE via 2-BENZOYL-1,2-DIHYDROISOQUINALDONITRILES: 1-BENZYLISOQUINOLINE [19]
ALLYLIC OXIDATION WITH HYDROGEN PEROXIDE-SELENIUM DIOXIDE: trans-PINOCARVEOL [25]
CARBOXYLATION OF AROMATIC COMPOUNDS: FERBOCENECARBOXYLIC ACID [28]
CHAIN ELONGATION OP ALKENES via gem-DIHALOCYCLOPROPANES: 1,1-DIPHENYL-2-BROMO-3-ACETOXY-1-PROPENE [32]
CONVERSION OF NITRO то CARBONYL BY OZONOLYSIS OF NITRONATES: 2,5-HEPTANEDIONE [36]
CONVERSION OF PRIMARY ALCOHOLS TO URETHANES (?) THE INNER SALT OF METHYL (CARBOXYSULFAMOYL)TRIETHYLAMMONIUM HYDROXIDE: METHYL (?)-HEXYLCARBAMATE [40]
DeMETHYLATION of METHYL ARYL ETHERS: 4-ETHOXY-3-HYDROXYBENZALDEHYDE [44]
5,6-DIHYDRO-2H-PYRAN-2-ONE AND 2H-PYRAN-2-ONE [49]
ENONE EEDUCTION-ENOLATE ALKYLATION SEQUENCE: 2-ALLYL-3-METHYLCYCLOHEXANONE [52]
ESTERIFICATION OF CARBOXYLIC ACIDS WITH TRIALKYLOXONIUM SALTS: ETHYL AND METHYL 4-ACETOXYBENZOATES [59]
ETHYL (E)-3-NITROACRYLATE [65]
FRЕЕ-RADICAL ALKYLATION OF QUINONES: 2-PHENOXYMETHYL-1,4-BENZOQUINONE [68]
INDOLES FROM ANILINES: ETHYL 2-METHYLINDOLE-5-CARBOXYLATE [72]
trans-IODOPROPENYLATION OF ALKYL, HALIDES: (E)-IODO-4-PHENYL-2-BUTENE [77]
METHYL GROUPS BY REDUCTION OF AROMATIC CARBOXYLIC ACIDS WITH TRICHLOROSILANE-TRI-(?)-PROPYLAMINE: 2-METHYLBIPHENYL [83]
PEPTIDE SYNTHESES USING N-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULFONATE: CARBOBENZOXY-L-ASPARAGINYL-L-LEUCINE METHYL ESTER AND N-CARBOBENZOXY-3-HYDROXY-L-PBOLYLGLYCYLGLYCINE ETHYL ESTER [88]
POLYMERIC CARBODIIMIDE. I. PREPARATION [95]
POLYMERIC CARBODIIMIDE. II. MOFFAT OXIDATION: 4-tert-BUTYLCYCLO-HEXANONE [99]
REDUCTIVE CLEAVAGE OF ALLYLIC ALCOHOLS, ETHERS, OR ACETATES TO OLEFINS: 3-METHYLCYCLOHEXENE [101]
RING CONTRACTION via (?) FAVORSK(?-TYPE REARRANGEMENT: CYCLOUNDECANONE [107]
SELECTIVE EPOXIDATION OF TERMINAL DOUBLE BONDS: 10,11-EPOXYFARNESYL ACETATE [112]
2,3,4,5-TETRAHYDHOPYRIDINE [118]
TRIFLUOROACETYLATION OF AMINES AND AMINO ACIDS UNDER NEUTRAL, MILD CONDITIONS- N-TRIFLUOROACETANILIDE AND N-ТRIFLUOROACETYL-L-TYROSINE [122]
AMINOACETONE SEMICARBAZONE HYDROCHLORIDE (CORRECTION) [127]
IODOMETHANE (WARNING) [127]
OSHA LIST OF CARCINOGENS (WARNING) [128]
AUTHOR INDEX [129]
SUBJECT INDEX [131]
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