Organic syntheses. V. 79, 2002

Автор(ы):Журнал
06.10.2007
Год изд.:2002
Описание: Семьдесят девятый номер брошюры «Органический синтез» содержит описания следующих соединений: SYNTHESIS OF TRIS(2-PERFLUOROHEXYLETHYL)TIN HYDRIDE: A HIGHLY FLUORINATED TIN HYDRIDE WITH ADVANTAGEOUS FEATURES OF EASY PURIFICATION; 1,2-METALLATE REARRANGEMENT:(Z)-4-(2-PROPENYL)-3-OCTEN-1-OL; DIMETHYLTITANOCENE; MOLYBDENUM CARBONYL-CATALYZED ALKYNOL CYCLOISOMERIZATION: PREPARATION OF 2-PHENYL-2,3-DIHYDROFURAN; ETHYL 3-(p-CYANOPHENYL)PROPIONATE FROM ETHYL 3-IODOPROPIONATE AND p-CYANOPHENYLZINC BROMIDE; PREPARATION OF n-BUTYL 4-CHLOROPHENYL SULFIDE; SYNTHESIS OF SYMMETRICAL frans-STILBENES BY A DOUBLE HECK REACTION OF (ARYLAZO)AMINES WITH VINYLTRIETHOXYSILANE: trans-4,4'-DIBROMOSTILBENE; SYNTHESIS AND UTILIZATION OF Inl FOR IN SITU FORMATION OF ENANTIOENRICHED ALLENYLINDIUM REAGENTS AND THEIR ADDITION TO ALDEHYDES: (2R,3S,4S)-1-(tert-BUTYLDIPHENYLSILYLOXY)-2,4-DIMETHYL-5-HEXYN-3-OL; ASYMMETRIC SYNTHESIS OF (M)-2-HYDROXYMETHYL-1-(2-HYDROXY-4,6-DIMETHYLPHENYL)NAPHTHALENE VIA A CONFIGURATIONALLY UNSTABLE BIARYL LACTONE. И некоторые другие. Всего рассмотрено 30 соединений.
Оглавление:
Organic syntheses. V. 79, 2002 — обложка книги.
SYNTHESIS OF TRIS(2-PERFLUOROHEXYLETHYL)TIN HYDRIDE: A HIGHLY FLUORINATED TIN HYDRIDE WITH ADVANTAGEOUS FEATURES OF EASY PURIFICATION [1]
  Aimee Crombie, Sun-Young Kim, Sabine Hadida, and Dennis P. Curran
1,2-METALLATE REARRANGEMENT:(Z)-4-(2-PROPENYL)-3-OCTEN-1-OL [11]
  Krzysztof Jarowicki, Philip J. Kocienski, and Liu Qun
DIMETHYLTITANOCENE [19]
  Joseph F. Payack, David L. Hughes, Dongwei Cai, Ian F. Cottrell, and Thomas R. Verhoeven
MOLYBDENUM CARBONYL-CATALYZED ALKYNOL CYCLOISOMERIZATION: PREPARATION OF 2-PHENYL-2,3-DIHYDROFURAN [27]
  Frank E. McDonald and Brian H. White
ETHYL 3-(p-CYANOPHENYL)PROPIONATE FROM ETHYL 3-IODOPROPIONATE AND p-CYANOPHENYLZINC BROMIDE [35]
  Anne Eeg Jensen, Florian Kneisel, and Paul Knochel
PREPARATION OF n-BUTYL 4-CHLOROPHENYL SULFIDE [43]
  J. Christopher McWilliams, Fred J. Fleitz, Nan Zheng, and Joseph D. Armstrong III
SYNTHESIS OF SYMMETRICAL frans-STILBENES BY A DOUBLE HECK REACTION OF (ARYLAZO)AMINES WITH VINYLTRIETHOXYSILANE: trans-4,4'-DIBROMOSTILBENE [52]
  Saumitra Sengupta and Subir K. Sadhukhan
SYNTHESIS AND UTILIZATION OF Inl FOR IN SITU FORMATION OF ENANTIOENRICHED ALLENYLINDIUM REAGENTS AND THEIR ADDITION TO ALDEHYDES: (2R,3S,4S)-1-(tert-BUTYLDIPHENYLSILYLOXY)-2,4-DIMETHYL-5-HEXYN-3-OL [59]
  Brian A. Johns, Charsetta M. Grant, and James A. Marshall
ASYMMETRIC SYNTHESIS OF (M)-2-HYDROXYMETHYL-1-(2-HYDROXY-4,6-DIMETHYLPHENYL)NAPHTHALENE VIA A CONFIGURATIONALLY UNSTABLE BIARYL LACTONE [72]
  Gerhard Bringmann, Matthias Breuning, Petra Henschel, and Jurgen Hinrichs
(R)-3-PHENYLCYCLOHEXANONE [84]
  Tamio Hayashi, Makoto Takahashi, Yoshiaki Takaya, and Masamichi Ogasawara
SYNTHESIS OF (+)-(1S,2R)-AND(-)-(1R,2S)-trans-2-PHENYLCYCLOHEXANOL VIA SHARPLESS ASYMMETRIC DIHYDROXYLATION (AD) [93]
  Javier Gonzalez, Christine Aurigemma, and Larry Truesdale
DICYCLOHEXYLBORON TRIFLUOROMETHANESULFONATE [103]
  Atushi Abiko
2-(N-BENZYL-N-MESITYLENESULFONYL)AMINO-1-PHENYL-1-PROPYLPROPIONATE [109]
  Atushi Abiko
ANTI-SELECTIVE BORON-MEDIATED ASYMMETRIC ALDOL REACTION OF CARBOXYLIC ESTERS: SYNTHESIS OF (2S,3R)-2,4-DIMETHYL-1,3-PENTANEDIOL [116]
  Atushi Abiko
CAMPHORQUINONE AND CAMPHORQUINONE MONOXIME [125]
  James D. White, Duncan J. Wardrop, and Kurt F. Sundermann
(2S)-(-)-3-exo(DIMETHYLAMINO)ISOBORNEOL [(2S)-(-)-DAIB] [130]
  James D. White, Duncan J. Wardrop, and Kurt F. Sundermann
CATALYTIC ENANTIOSELECTIVE ADDITION OF DIALKYLZINCS TO ALDEHYDES USING (2S)-(-)-3-exo-(DIMETHYLAMINO)ISOBORNEOL [(2S-DAIB]: (S)-1-PHENYL-1-PROPANOL [139]
  Masato Kitamura, Hiromasa Oka, Seiji Suga, and Ryoji Noyori
FORMATION OF y-KETO ESTERS FROM (?)-KETO ESTERS: METHYL 5,5-DIMETHYL-4-OXOHEXANOATE [146]
  Matthew D. Ronsheim, Ramona K. Hilgenkamp, and Charles K. Zercher
(S)-3-(tert-BUTYLOXYCARBONYLAMINO)-4-PHENYLBUTANOIC ACID [154]
  Michael R. Under, Steffen Steurer, and Joachim Podlech
PHOTO-INDUCED RING EXPANSION OF 1-TRIISOPROPYLSILYLOXY-1-AZIDOCYCLOHEXANE: PREPARATION OF (?)-CAPROCACTAM [165]
  Jade D. Nelson, Dilip P. Modi, and P. Andrew Evans
(3,4,5-TRIFLUOROPHENYL)BORONIC ACID-CATALYZED AMIDE FORMATION FROM CARBOXYLIC ACIDS AND AMINES: N-BENZYL-4-PHENYLBUTYRAMIDE [176]
  Kazuaki Ishihara, Suguru Ohara, and Hisashi Yamamoto
PREPARATION OF SECONDARY AMINES FROM PRIMARY AMINES VIA 2-NITROBENZENESULFONAMIDES: N-(4-METHOXYBENZYL)-3-PHENYLPROPYLAMINE [186]
  Wataru Kurosawa, Toshiyuki Kan, and Tohru Fukuyama
2-AMINO-3-FLUOROBENZOIC ACID [196]
  Martin Kollmar, Richard Parlitz, Stephan R. Oevers, and Gunter Helmchen
3-(4-BROMOBENZOYL)PROPANOIC ACID [204]
  Alexander J. Seed, Vaishali Sonpatki, and Mark R. Herbert
NUCLEOPHILIC AROMATIC SUBSTITUTION OF ARYL FLUORIDES BY SECONDARY NITRILES: PREPARATION OF 2-(2-METHOXYPHENYL)-2-METHYLPROPIONITRILE [209]
  Stephane Caron, Jill M. Wojcik, and Enrique Vazquez
PREPARATION OF 1-[N-BENZYLOXYCARBONYL-(1S)-1-AMINO-2-OXOETHYL]-4-METHYL-2,6,7-TRIOXABICYCLO[2.2.2]OCTANE [216]
  Nicholas G.W. Rose, Mark A. Blaskovich, Ghotas Evindar, Scott Wilkinson, Yue Luo, Dan Fishlock, Chris Reid, and Gilles A. Lajoie
N-HYDROXY-4-(p-CHLOROPHENYL)THIAZOLE-2(3H)-THIONE [228]
  Jens Hartung and Michaela Schwarz
PREPARATION OF 1-BUTYL-3-METHYL IMIDAZOLIUM-BASED ROOM TEMPERATURE IONIC LIQUIDS [236]
  Jairton Dupont, Crestina S. Consorti, Paulo A.Z. Suarez, and Roberto Fe de Souza
4-METHOXYCARBONYL-2-METHYL-1,3-OXAZOLE [244]
  James D. White, Christian L. Kranemann, and Punlop Kuntiyong
[4+3] CYCLOADDITION IN WATER SYNTHESIS OF 2,4-endo, endo-DIMETHYL-8-OXABICYCLO[3.2.1]OCT-6-EN-3-ONE [251]
  Mark Lautens and Giliane Bouchain
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